L-2-Nitrimino-1,3-diazepane-4-carboxylic acid

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l-2-Nitrimino-1,3-diazepane-4-carboxylic acid monohydrate

The cyclic form of l-nitro-arginine, C(6)H(10)N(4)O(4), crystallizes with two independent mol-ecules in the asymmetric unit. According to the geometrical parameters, similar in both mol-ecules, the structure corresponds to that of l-2-nitrimino-1,3-diazepane-4-carboxylic acid; there are, however, conformational differences between the independent molecules, one of them being close to a twisted ...

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Potassium l-2-nitrimino-1,3-diazepane-4-carboxyl­ate monohydrate

The title compound, K(+)·C(6)H(9)N(4)O(4) (-)·H(2)O, crystallizes with the K atoms located on special positions related by pseudocentres of symmetry. Each K atom is coordinated by six O-atom donors. The N and water H atoms are involved in inter- and intra-molecular N-H⋯O, N-H⋯N and O-H⋯O hydrogen bonding. The data indicate inversion twinning.

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L-2-[(13)C]oxothiazolidine-4-carboxylic acid: a probe for precursor mobilization for glutathione synthesis.

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6-Fluoro-4-oxochroman-2-carboxylic acid

The title compound, C(10)H(7)FO(4), is an inter-mediate in the synthesis of the drug Fidarestat, (2S,4S)-2-aminoformyl-6-fluoro-spiro[chroman-4,4'-imidazolidine]-2',5'-dione. The di-hydro-pyran-one ring adopts an envelope conformation with the asymmetric C atom in the flap position. In the crystal, the mol-ecules are linked into zigzag chains along [100] by O-H⋯O hydrogen bonds and C-H⋯π inter-...

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SYNTHESIS OF 3-ARYLMETHYL-4- THIAZOLIDINE-CARBOXYLIC ACID-2-ONES AND 2-THIONES

Barium salts of dibenzylidene cystines 8a-c were obtained from the reaction of Lcystine with benzaldehyde or its derivatives in the presence of barium hydroxide. Their reduction with zinc and hydrochloric acid in methanol yielded the Narylmethylcysteines ?9a-c?. These can, in turn, be converted by esterification into the methyl esters ?10 a-c. ?Reaction of N, N'-carbonyl diimidazole (Im C...

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ژورنال

عنوان ژورنال: Acta Crystallographica Section E Structure Reports Online

سال: 2008

ISSN: 1600-5368

DOI: 10.1107/s1600536808011835